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Does anyone know what the term "mole percent" would appropriately based on in this case?Ġ.51 mmol (phenol der.) + 1.0 mmol (aldehyde) + x mol PhB(OH)2 + y mol PhCOOH = z total molĠ.51 mmol (phenol der.) + 1.0 mmol (aldehyde) + 0.2z + 0.05z = z total molĠ.05 (2.013) = 0.10 mol phenyl boric acid It makes most sense that the mole percent for this protocol would be based on the limiting reagent, but I included the calculations based on the total moles of reactants and catalysts for reference. There are many different interpretations of this I have seen online, including mole percent being based on a fraction of the limiting reagent (the phenol in this case), the mole percent being based on the fraction of all of the total moles of reactant and catalyst (most fitting of the definition of mole percent), and the mole percent being based on all of the moles of reactant, catalyst, and solvent. I am trying to figure out what is meant by mole% in this case. The paper calls for 0.51 mmol of 3,5-dimethoxy phenol, 1.0 mmol of 3-methyl-3-butenal, 5 mol% of phenylboronic acid, 20 mol% of benzoic acid, and 2.5 mL of heptane. I am attempting to interpret an experimental section on a scientific paper.
